การสร้าง Calibration Curve สา หรับห

Create a Calibration Curve for nok ongsan mok determine eternal dissolved ethanol. 1. prepare a standard ethanol aqueous solution at a concentration of 10% 5% 0% 20% 30% 40% 50% 60% 70% 80% 85% 90% 95% and 99.8% by volume from ethanol lakhem 99.8% each 10 ml condensed 2. na solution, the concentration to Refractive index with a Refractometer na วดัค่า. Ethanol aqueous solution lakhem concentrate 80% 85% 90% 95% and 99.8% by volume to find density using a Pycnometer. Passing West rough standard curve shows the relationship between Refractive index with an eternal value nok ongsan mok dissolved ethanol (v%) for ethanol aqueous solution that demands an eternal and mok น้ต่ากว่า 80% of the meaning of the Refractive index with the พนัธ์ function set the density values of aqueous solution. Ethanol (g/cm3) for the meanings of the TA mok nok onge crossed through 80% ตน้ to latangtae. Episode 2-up Start 1. prepare solution ethanol at 10%, by volume – eternal mok & 200 litre Java from aqueous solution. 95% ethanol by volume 2. study of the components of the spear at one all. In order to write P&ID NA (Piping and instrumentation diagram). 17. 3. turn on main switch and switch pump feed 4. open valve (No. 1) to slurry tank (tank feed) to slurry enters the reboiler by a notice from the internal lights, colors, creative Finance Panel will display the quantity of creative within the reboiler Heat Supply and adjust 5. open season ง้ไฟฟ้า SA. For a hot start ตน้ ค้วาม between a 11 kW cooling water open to 6. preparation the condenser heat exchanger 7. TA value adjustment in the system: flow rate flow rate, feed and reflux heating rate to hairabop into a fixed one Council WA. (Steady state) 8. ตวัอ liquid storage Grill each 10 ml at all 6 trays (valve, no. 10-15), where all the packing bed 2 points (16-17 number wan) and distillate 1. (Wan number 27) total 9 points 9. na ตวัอ Yang collected liquid to วดัค่า to find the refractive index of the solution concentration ethanol or wadak of density. When mok น้สูงเกิน crossed 80% when compared to the calibration curve built 10. วดัอ ตัราการ flow of distillate that can be refined. Episode 3 of the impact studies added to summer heating rate อตัราการให ค้วาม. 1. บนัทึกข อ้มูลตอน ตน้ที่ feed flow rate 40 l starts/h, l/h flow rate 17 reflux and 11 kW heating rate 2. Ta add only hot (heating rate) อตัราการให ค้วาม haimikha 13 3 kW. to observe the changes of temperature, both 10 points (T-101 to T-112) 4. TA value adjustment of flow rate in the system is sufficiently feed flow rate and heating rate, the reflux to attend Council of WA, fixed one. (Steady state) 5., and then store the liquid ตวัอ total 9 points to grill, as well as the experimental part 2 analyzed for NA. Determine the functionality of the Ethanol distillation crossed mok nok. 6. วดัอ ตัราการ flow of Ethanol can be distilled anhydrous thi Reflux Drum yadu smearing. The job of the Spears to pull continuous layers

Creating Calibration Curve For the messages for the solution of ethanol 1. Prepare a standard solution of ethanol. 0% 5% at a concentration of 10% 20% 30% 40% 50% 60% 70% 80% 85% 90% 95% and 99.8% by volume of ethanol concentration of 99.8% as per 10 ml 2. appropriate. Each solution is the concentration of the industry Refractometer Refractive index with a solution of ethanol concentration 80%, 85%, 90%, 95% and 99.8% by volume to determine the density using Pycnometer 3. Plot. standard curve shows the relationship between the Refractive index on the cost of the messages of the solution of ethanol (% v) for the solution of ethanol at concentrations obtained little less than 80% and their properties. E for heavy bandwidth between the Refractive index and the density of the aqueous solution of ethanol (g / cm3) for the incoming messages of ethanol from 80% in the next episode 2 Start - up 1. . Prepare a solution of ethanol. The concentrations obtained with 10% volume Quantity 200 liters of a solution of ethanol 95% by volume 2. The components of the tower and all friends of the writing P & ID (Piping and Instrumentation diagram)
17
3. Open the main switch. and switch pump feed 4. Open the valve (number 1) The solution tanks (feed tank) to enter the solution into the reboiler by observing the color of light. Repeat the control panel will show the amount of water in the reboiler 5. Open Heat Supply and adjusted net electricity in me for so valued less hot start is 11 kW 6. Preparation for open cooling water heat exchanger condenser. 7. Distribution of adjustments within the system include a feed flow rate, reflux flow rate and the heating rate to the AMC into the Oval steady state (steady state) 8. Collect liquid with Valvoline each 10 ml all the trays. 6 points (valve No. 10-15), the packing bed all two points (valve No. 16-17) and distillate 1 point (valve No. 27) totaled 9 points 9. The liquid is collected through the valley. to provide that the refractive index to determine the concentration. Ethanol solution Or the Dutch density If high concentrations obtained more than 80% compared to a calibration curve generated by the industry in each mold 10. The flow of distillate that can be refined
at the three studied the effects of adding each mold so valued. Hot Heating rate
Terminal 1. The record info page at the beginning of the feed flow rate 40 l / h., reflux flow rate 17 l / h. and heating rate 11 kW 2. The adding each particular mold of the year. Another hot (heating rate) to 13 kW 3. The observed changes in temperature as 10 points (T-101 and T-112) 4. The adjustments within the system, namely feed flow rate, reflux flow rate. and the heating rate to a steady-state system into the Oval (steady state) 5. Then keep liquid Valle at all nine points as the two trials analyzed to determine the concentration of Ethanol is distilled rice. 6. The Dutch de Chantal mold flow Ethanol can be distilled at a fierce Reflux Drum 7. The operation of the multi-layer distillation.

The Calibration Curve SA for the reliability เขม้ fur of ethanol solution 1. Prepare standard solution of ethanol concentration. 0% 5% 10% 20% 30% 40% 50% 60% 70% 80% 85% and 90% 95% 99.8% by volume. From ethanol concentration 99.8% each 10 ml 2.. each solution concentration ไปวดั value Refractive index machine with Refractometer. Ethanol solution concentration and 80% 85% 90% 95% 99.8% by volume. To find the density as well, Pycnometer 3.Plot a graph standard curve shows the relationship between the Refractive index with the เขม้ fur of ethanol solution (%v) post for ethanol water solution and เขม้ fur per Than 80% and show สัมพนั associations between the Refractive index.Ethanol (g / cm3) SA for the เขม้ fur of ethanol from 80% is the, when 2 Start - up 1.Ethanol solution prepared at the เขม้ fur 10% River by volume. Hot number 200 L from aqueous solution of ethanol 95% by volume 2. To study the components of distillation column. Friend to write P & ID (Piping and instrumentation diagram)

3 17. Open and main switch switch pump feed 4.Open the valves (the number 1) contain the solution tank (feed tank) to enter into the interior reboiler solution by observation of blue lights, money control panel will show the quantity. Diving in reboiler 5.Open Heat Supply and fine, are then electricity industry for ใหค้ hot start their article is 11 kW 6. Open cooling water for the preparation of a heat exchanger. Condenser 7. Tom to adjust parameters within the system, namely, feed flow rateReflux and flow rate heating rate to ใหร้ system to a state. They have (steady state) 8. Keep liquid ตวั. Each 10 ml. Trays all 6 point number, 10-15 (valve)The packing bed all 2 points (vlave number 16-17) and distillate 1 points (vlave number 27) as well as the 9 points 9.. the liquid ตวั as luggage all ไปวดั value refractive index to determine the concentration of สารละลายเอทานอล or space trap density. If the เขม้ hair too high 80% compared with calibration curve made 10.วดั อตั recipe flow of distillate can still have
when 3 study the impact of the increase อตั recipe ใหค้ hot articles heating rate
1. Nut deep B om - Ultra at the beginning of the. Feed flow rate 40 L / h, reflux flow rate 17 l / h. And heating rate 11 kW 2.Apply to add specific อตั recipe ใหค้ hot articles (heating rate) on fire has the 13 kW 3. Observe the change of temperature, all of the 10 points (points T-101. To T-112) 4. Apply various adjustment within the system, and the construction of feed, flow rateReflux flow rate heating rate and to make the system he conditions. (steady state) have 5. Then keep liquid ตวั all 9 points as well as the experiment when 2 friends. To analyze the reliability of เขม้ fur Ethanol distilled has 6.วดั อตั recipe flow of Ethanol can be distilled ไดท้ that Reflux Drum 7. Hold the work of continuous distillation of several layers.