TMS as internal standard. 1H–1H COS

TMS as internal standard. 1H–1H COSY, HSQC,
HMBC and NOESY (500 ms mixing time) were
obtained using the standard pulse sequences. ESITOFMS
and ESI-MS/MS were recorded in positive
mode on a API Q-STAR PULSA of Applied Bio-system.
CC was carried out on silica gel (Acme) finer than
200 mesh (0.08 mm)

ผลลัพธ์ (อังกฤษ) 2:

TMS as internal standard. 1H-1H COSY, HSQC,
HMBC and NOESY (mixing time 500 MS) were
obtained using standard The Pulse sequences. ESITOFMS
and ESI-MS / MS were positive Recorded in
API Mode on a Q-STAR PULSA of Applied Bio-System.
CC was carried out on Silica gel (Acme) Finer than
200 mesh (12:08 mm).