Device consists of the extraction of 20mg Sorbents from Pall packed
Inside a (1.5 cm × 1.5 cm) porous polypropylene membrane Envelope
Made from whose Sheets Two overlapping open edges were
heat-sealed. The detailed fabrication of the Device has been
previously reported [32-34]. Each Device was cleaned by ultrasonication
in methanol for 10min. It was then stored in the
Clean methanol until use. The? -SPE Device was Placed in a
soil sample (20 G with 15 ml of ultrapure Water, pH was not
adjusted and no Salt was added) that was stirred at ca. RAD 105 s-1
(the 1,000th RPM; 1rpm RAD = 0.1047 s-1). After extraction (90 min), the
Device was removed, rinsed in ultrapure Water, dabbed Dry with
a lint-free tissue and Placed in 200? L crimper Vial. The analytes
were Desorbed by ultrasonication in acetonitrile (150? L) and the
100? L Extract was injected directly Into the HPLC for Analysis.
The? -SPE Device could be reused after with the Same Cleaning
Solvent.
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