A single phase microemulsion was pr

A single phase microemulsion was prepared from 7.5 g of 1,2-dichloroethane (1,2-DCE, Sigma-Aldrich 99%), 5 g of Millipore MQ water and 6 g of sodium dihexylsulfosuccinate (SDHSS, Aldrich, 80% in H2O), corresponding to a final composition of 41:33:26 wt.% (1,2-DCE:W:SDHSS). 0.02 g of decamethylferrocene (DcMFc, Aldrich 97%) was added to the microemulsion and the solution purged with nitrogen. 0.36 g of LiTPBF20 (Boulder) or 1.21 g of tetrabutylammonium chloride (TBACl, Aldrich 97%) was added to 3.1 g of microemulsion. The potential between a Pt wire and a SCE electrode was recorded using a CH Instruments potentiostat while the TBACl or LiTPBF20 containing microemulsion was titrated into 3.1 g of microemulsion under vigorous mixing. The electrochemical cell was:

ผลลัพธ์ (แอฟริกา) 1:

'N enkel fase micro is bereid om van 7,5 g van 1,2-dichloroethane (1,2-DCE, Sigma-Aldrich 99%), 5 g van Millipore MQ water en 6 g van natrium dihexylsulfosuccinate (SDHSS, Aldrich, 80% in H2O. ), wat ooreenstem met 'n finale samestelling van 41:33:26 wt% (1,2-DCE. W: SDHSS). 0,02 g van decamethylferrocene (DcMFc, Aldrich 97%) is by die micro en die oplossing versoen met stikstof. 0,36 g van LiTPBF20 (Boulder) of 1.21 g van tetrabutylammonium chloried (TBACl, Aldrich 97%) is bygevoeg tot 3,1 g van micro. Die potensiaal tussen 'n Pt draad en 'n SCE elektrode is aangeteken met behulp van 'n CH-instrumente potentiostaat terwyl die TBACl of LiTPBF20 met micro getitreer in 3.1 g van micro onder kragtige vermenging. Die elektrochemiese sel was: