The column temperature was maintained at 50 ◦C for 2 min. Then the
temperature was elevated to 110 at 10 ◦Cmin−1 and finally
to 200 ◦C at 5 ◦Cmin−1. Mass numbers between 30 and 550
(m/z) were recorded. There was an error in the procedure
of making the extraction solutions, thus the extraction solution
used for the Splendid leaves contained an extremely
high concentration of the internal standard (1-chloro-octane)